Home Cart Sign in  
Chemical Structure| 913629-79-5 Chemical Structure| 913629-79-5

Structure of 913629-79-5

Chemical Structure| 913629-79-5

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 913629-79-5 ]

CAS No. :913629-79-5
Formula : C6H4BrFO2
M.W : 207.00
SMILES Code : OC1=CC(F)=CC(Br)=C1O

Safety of [ 913629-79-5 ]

Application In Synthesis of [ 913629-79-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 913629-79-5 ]

[ 913629-79-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 178546-34-4 ]
  • [ 913629-79-5 ]
YieldReaction ConditionsOperation in experiment
74% With dihydrogen peroxide; sodium hydroxide; In water; at 20℃; for 2h; Weigh 30-2 (350mg, 1.6mmol) A solution of sodium hydroxide (83 mg, 2.08 mmol) in water (5 mL). Then a solution of hydrogen peroxide (190 muL, 6.18 mmol) in water (5 mL) was slowly added dropwise. The system was reacted at room temperature for 2h. After the reaction, the system was adjusted to pH = 1 with a 1N hydrochloric acid solution, and the aqueous phase was extracted with ethyl acetate (20 mL x 2). The organic phases were combined, and the organic phase was washed with saturated brine (10 mL x 1). Dry over anhydrous sodium sulfate and evaporate the solvent under reduced pressure. The residue was purified by column chromatography (eluent: petroleum ether / ethyl acetate = 10: 1-8: 1), Compound 30-3 (yellow solid, 258 mg) was obtained.
 

Historical Records