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Chemical Structure| 91319-42-5 Chemical Structure| 91319-42-5

Structure of 91319-42-5

Chemical Structure| 91319-42-5

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Product Details of [ 91319-42-5 ]

CAS No. :91319-42-5
Formula : C8H8BrFO
M.W : 219.05
SMILES Code : COC1=CC=C(F)C(CBr)=C1
MDL No. :MFCD11617285

Safety of [ 91319-42-5 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H314
Precautionary Statements:P280-P305+P351+P338-P310
Class:8
UN#:1759
Packing Group:

Application In Synthesis of [ 91319-42-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 91319-42-5 ]

[ 91319-42-5 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 2338-54-7 ]
  • [ 91319-42-5 ]
YieldReaction ConditionsOperation in experiment
With N-Bromosuccinimide; Perbenzoic acid; In tetrachloromethane; for 2h;Reflux; To a solution of l-fluoro-4-methoxy-2-methylbenzene (2.0 g, 14.29 mmol) in CC , NBS (2.55 g, 14.29 mmol) and PI1CO3H (80 mg) were added. The reaction mixture was heated at reflux for 2 h, cooled to room temperature, and the solid was filtered off. The filtrate was concentrated, and the residue was purified by silica gel column chromatography (eluting with PE/EA = 20/1) to give the target compound (3.0 g) as an oil. 1H NMR (CDC13): δ 6.97-6.83 (m, 3H), 4.48 (s, 2H), 3.78 (s, 3H).
  • 2
  • [ 91319-42-5 ]
  • [ 119838-38-9 ]
  • tert-butyl (2S,5S)-2-(tert-butyl)-5-(2-fluoro-5-methoxybenzyl)-3-methyl-4-oxo-1-imidazolidinecarboxylate [ No CAS ]
 

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