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Chemical Structure| 909912-09-0 Chemical Structure| 909912-09-0

Structure of 909912-09-0

Chemical Structure| 909912-09-0

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Product Details of [ 909912-09-0 ]

CAS No. :909912-09-0
Formula : C15H15NO4
M.W : 273.28
SMILES Code : O=C(O)C1=CC(OCC2=CC=CC=C2)=C(OC)C=C1N

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Application In Synthesis of [ 909912-09-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 909912-09-0 ]

[ 909912-09-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 909912-09-0 ]
  • [ 3473-63-0 ]
  • [ 286371-64-0 ]
YieldReaction ConditionsOperation in experiment
94% 6-(benzyloxy)-7-methoxyquinazolin-4(3H)-one: Preparation 9 (5 g,18.3 mmol) was mixed with amidine acetate (3.8 g, 36.6 mmol) in ethylene glycol monomethyl ether (25 mL) and the mixture was heated at 13O0C for 24 h. After cooling to room temperature, part of the solvent was removed in vacuo and ammonium hydroxide (5 mL, 30% in water) and water (50 mL) were added. The solid was filtered, was washed with water and hexanes, and was then dried under vacuum to afford 4.87 g (94% yield) of the title compound; MS (AP/CI): 283.1 (M+H)+ .
 

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