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Chemical Structure| 90918-37-9 Chemical Structure| 90918-37-9

Structure of 90918-37-9

Chemical Structure| 90918-37-9

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Product Details of [ 90918-37-9 ]

CAS No. :90918-37-9
Formula : C10H12N2O2
M.W : 192.21
SMILES Code : O=C(C1=CC2=C(NCCN2)C=C1)OC
MDL No. :MFCD18252992

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 90918-37-9 ]

[ 90918-37-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 23088-23-5 ]
  • [ 90918-37-9 ]
YieldReaction ConditionsOperation in experiment
87% With sodium tetrahydridoborate; In methanol; at 90.0℃; for 2.0h; Take a 100 ml single-mouth bottle, add quinoxaline-6-carboxylic acid methyl ester (3) 3.76 g (0.02 mol), add 50 ml of methanol, stir to dissolve,Then, 3.02 g (0.08 mol) of sodium borohydride was slowly added.The reaction was carried out at 90 C for 2 hours.After the reaction is completed, excess methanol is distilled off under reduced pressure.Then, it is extracted and dried to obtain 3.24 g of methyl 1,2,3,4-tetrahydroquinoxaline-6-carboxylate (4).The yield was 87%.
 

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