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Chemical Structure| 89364-41-0 Chemical Structure| 89364-41-0

Structure of 89364-41-0

Chemical Structure| 89364-41-0

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Product Details of [ 89364-41-0 ]

CAS No. :89364-41-0
Formula : C5H8O4
M.W : 132.11
SMILES Code : O=C(C1OCCOC1)O
MDL No. :MFCD06260725
Boiling Point : No data available
InChI Key :VGBAYGFELCUXBS-UHFFFAOYSA-N
Pubchem ID :5230755

Safety of [ 89364-41-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 89364-41-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 89364-41-0 ]

[ 89364-41-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 89364-41-0 ]
  • [ 1121057-75-7 ]
  • 1,4-dioxane-2-yl-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,6-dihydropyridin-1(2H)-yl]methanone [ No CAS ]
YieldReaction ConditionsOperation in experiment
2.3 g 1,2,3,6-tetrahydro pyridin-4-yl-boron acid Triethylamine (2.84 mL) is added to the N.N-dimethylformamide (20 mL) solution of pinacol ester salt acid chloride (CAS number: 1121057-75-7) (2.50 g), It stirred for 5 minutes at the room temperature. 4-(4,6-dimethoxy- 1,3,5-triazine 2-yl)-4-methylmorpholinium Chloride (4.20 g) and 1,4-dioxane 2-carboxylic acid (1.61 g) was added, and it stirred at the room temperature for 18 hours. Water was added to reaction mixture, the organic layer was washed twice with water after extraction with ethyl acetate, and the saturated sodium chloride solution washed further. After drying with anhydrous sodium sulfate, the mark compound (2.30 g) was obtained as a brown oily matter by condensing under decompression.
 

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