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Chemical Structure| 87080-27-1 Chemical Structure| 87080-27-1

Structure of 87080-27-1

Chemical Structure| 87080-27-1

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Product Details of [ 87080-27-1 ]

CAS No. :87080-27-1
Formula : C21H22O4
M.W : 338.40
SMILES Code : O=C(C1=CC=C(O)C=C1)C=CC2=CC(C(C)(C)C=C)=C(O)C=C2OC
MDL No. :N/A

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Application In Synthesis of [ 87080-27-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 87080-27-1 ]

[ 87080-27-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 87080-27-1 ]
  • [ 5637-42-3 ]
  • 4-(6-(4-hydroxy-2-methoxy-5-(2-methylbut-3-en-2-yl)phenyl)-4-(4-hydroxyphenyl)-2-imino-5,6-dihydropyridine-1(2H)-yl)benzonitrile [ No CAS ]
YieldReaction ConditionsOperation in experiment
49.44% With triethylamine; In ethanol; at 75℃; for 6h; To the reactor is added in the licorice chalcone A200mg (1mmol) and 1 - (4 - cyano phenyl) guanidine 123.07 mg (1.3mmol), adding 50 ml ethanol as solvent, adding 0.5 ml triethylamine as catalyst, placed over the magnetic stirrer stirring, heated to 75 C, reflux reaction for 6 hours. In the reaction process using thin layer chromatography tracking, monitoring the reaction in a timely manner the intensity, the raw materials after the reaction is complete cessation of heating, condensing device is removed. The mixture of the reaction system was concentrated under reduced pressure, filtration, column chromatography separation and purification, drying to obtain the target product 140.42 mg, yield is 49.44%.
 

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