870-78-0|Diethyl 2,4-dibromopentanedioate| Ambeed

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Quality Control of [ 870-78-0 ] Purity: 95% SDS Specification

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Product Details of [ 870-78-0 ]

CAS No. :	870-78-0
Formula :	C₉H₁₄Br₂O₄
M.W :	346.01
SMILES Code :	O=C(OCC)C(Br)CC(Br)C(OCC)=O
MDL No. :	MFCD31697873
InChI Key :	DUSLEJGELFKEAS-UHFFFAOYSA-N
Pubchem ID :	12463730

Safety of [ 870-78-0 ]

GHS Pictogram:
Signal Word:	Warning
Hazard Statements:	H302-H315-H319-H335
Precautionary Statements:	P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 870-78-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 870-78-0 ]

[ 870-78-0 ] Synthesis Path-Downstream 1~35

1
[ 870-78-0 ]
[ 103-85-5 ]
2,2'-diimino-3,3'-diphenyl-5,5'-methanediyl-bis-thiazolidin-4-one [ No CAS ]

References: [1]Journal of the Chemical Society,1932,p. 1579.

2
[ 2873-74-7 ]
[ 64-17-5 ]
[ 870-78-0 ]

References: [1]Tetrahedron Asymmetry,1995,vol. 6,p. 2921 - 2924.

3
[ 870-78-0 ]
[ 100-46-9 ]
[ 1016233-19-4 ]
diethyl (2R*,4R*)-1-benzylazetidine-2,4-dicarboxylate [ No CAS ]

References: [1]Tetrahedron Asymmetry,1995,vol. 6,p. 2921 - 2924.
[2]Tetrahedron Asymmetry,2001,vol. 12,p. 605 - 618.
[3]Synthesis,2012,vol. 44,p. 2859 - 2862.

Yield	Reaction Conditions	Operation in experiment
52%	With bromine; In methanol; dichloromethane; at 0 - 20℃; for 8.0h;	General procedure: Dimethyl suberate (23.2 kg) was added to dichloromethane (200 kg), and after cooling to 0-10 C, liquid bromine (75 kg) was slowly added, and the addition was completed. The reaction was added to methanol (25 Kg) at room temperature. After 8 hours of cooling to 0 C, the solid was filtered off, and acetone was recrystallized to obtain pure product 2,7-dibromooctanedioic acid dimethyl ester 28 kg (yield 68%). .

6
[ 870-78-0 ]
[ 127310-66-1 ]

References: [1]Tetrahedron Asymmetry,2001,vol. 12,p. 605 - 618.
[2]Tetrahedron Asymmetry,1995,vol. 6,p. 2921 - 2924.

7
[ 870-78-0 ]
(±)-trans-(1-benzyl-azetidine-2,4-diyl)dimethanol [ No CAS ]

References: [1]Tetrahedron Asymmetry,2001,vol. 12,p. 605 - 618.
[2]Tetrahedron Asymmetry,1995,vol. 6,p. 2921 - 2924.

8
[ 870-78-0 ]
(2R*,4S*)-2,4-bis(acetoxymethyl)-1-benzylazetidine [ No CAS ]