Home Cart Sign in  
Chemical Structure| 84832-73-5 Chemical Structure| 84832-73-5

Structure of 84832-73-5

Chemical Structure| 84832-73-5

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 84832-73-5 ]

CAS No. :84832-73-5
Formula : C14H8Br2N2O
M.W : 380.03
SMILES Code : BrC1=CC(C2=NN=C(C3=CC=CC(Br)=C3)O2)=CC=C1
MDL No. :MFCD09394754
InChI Key :OLBIUUBQSQBMDC-UHFFFAOYSA-N
Pubchem ID :259341

Safety of [ 84832-73-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P210-P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P332+P313-P337+P313-P362-P370+P378-P403+P233-P403+P235-P405-P501

Application In Synthesis of [ 84832-73-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 84832-73-5 ]

[ 84832-73-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 870119-58-7 ]
  • [ 84832-73-5 ]
  • 2,5-bis(3'-(9H-carbazol-9-yl)biphenyl-3-yl)-1,3,4-oxadiazole [ No CAS ]
YieldReaction ConditionsOperation in experiment
80% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In ethanol; toluene; at 95℃; for 24h; To a 50 ml three-necked flask was added 2,5-bis- (3-bromophenyl) -1,3,4-oxadiazole D2 (0.95 g, 2.5 mmol), 9- (3- (4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl) phenyl) -9 hydrogen-carbazole (2.62 g, 7.1 mmol), 2MK2CO3Solution 16ml, tetraphenylphenylphosphine palladium (Pd (PPh)3)4) (90.0 mg, 0.08 mmol), toluene (80 ml) and ethanol (16 ml). The mixture was heated to 95 C and stirred for 24 h.After cooling to room temperature, add the appropriate amount of water to quench the reaction and dilute with dichloromethane (DCM). The organic phase was separated and the aqueous phase was extracted three times with DCM. The organic phases were combined and the organic layer was washed three times with saturated brine TheDried over anhydrous magnesium sulfate and filtered, and the resulting filtrate was removed under reduced pressure. The column was separated (1.40 g, 2.0 mmol) as a white solid with a yield of 80.0%.
 

Historical Records

Technical Information

Categories