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Chemical Structure| 847818-49-9 Chemical Structure| 847818-49-9

Structure of 847818-49-9

Chemical Structure| 847818-49-9

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Product Details of [ 847818-49-9 ]

CAS No. :847818-49-9
Formula : C6H9BrN2O
M.W : 205.05
SMILES Code : COCCN1N=CC(Br)=C1
MDL No. :MFCD12405645
InChI Key :SJIMZWZHTDHXRI-UHFFFAOYSA-N
Pubchem ID :23247855

Safety of [ 847818-49-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 847818-49-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 847818-49-9 ]

[ 847818-49-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 847818-49-9 ]
  • [ 847818-71-7 ]
  • 2
  • [ 73183-34-3 ]
  • [ 847818-49-9 ]
  • [ 847818-71-7 ]
YieldReaction ConditionsOperation in experiment
45% To the solution of 23b (0.61g, 2.97mmol) and bis(pinacolato)diboron (0.91g, 3.57mmol) in DMF (2OmL), was added KOAc (0.87g, 8.91mmol). The mixture was degassed with N2, stirred for 1 Omin and added Pd(dppf)Cl2. CH2Cl2 (73mg, 0.089mmol). The mixture was degassed with N2 and stirred at 8O0C overnight. After the reaction was complete, DMF was evaporated and the residue was purified by column chromatography (EA:PE=1 :7) to afford 23c (0.34g, 45percent yield) as oil.
 

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