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Chemical Structure| 83112-38-3 Chemical Structure| 83112-38-3

Structure of 83112-38-3

Chemical Structure| 83112-38-3

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Product Details of [ 83112-38-3 ]

CAS No. :83112-38-3
Formula : C10H12O4S
M.W : 228.26
SMILES Code : O=C(OCC)C1=CC=CC(S(=O)(C)=O)=C1
MDL No. :MFCD12025159

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Application In Synthesis of [ 83112-38-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 83112-38-3 ]

[ 83112-38-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 83112-38-3 ]
  • [ 220798-39-0 ]
YieldReaction ConditionsOperation in experiment
With lithium borohydride; In tetrahydrofuran; water; Reference Example 13 3-Methanesulfonylbenzyl alcohol Ethyl 3-methanesulfonylbenzoate (420 mg) was dissolved in 4 ml of tetrahydrofuran, 120 mg of lithium borohydride was added to the solution, and the mixture was heated under reflux for 20 hours under an argon atmosphere. Water was added to the reaction mixture, and the mixture was extracted with ethyl acetate. The organic layer was washed successively with a saturated aqueous sodium hydrogen carbonate solution and brine, and dried over anhydrous magnesium sulfate. The solvent was removed under reduced pressure to give 283 mg of 3-methanesulfonylbenzyl alcohol. 1H-NMR(CDCl3) delta ppm: 1.91 (1H, t, J=5.8Hz), 3.07 (3H, s), 4.82 (2H, d, J=5.8Hz), 7.57 (1H, t, J=7.7Hz), 7.67 (1H, d, J=7.7Hz), 7.87 (1H, d, J=7.7Hz), 7.97 (1H, s)
 

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