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Chemical Structure| 82964-91-8 Chemical Structure| 82964-91-8

Structure of 82964-91-8

Chemical Structure| 82964-91-8

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Product Details of [ 82964-91-8 ]

CAS No. :82964-91-8
Formula : C7H7ClO4S2
M.W : 254.71
SMILES Code : O=S(C1=CC=C(S(=O)(C)=O)C=C1)(Cl)=O
MDL No. :MFCD00216486
InChI Key :TYJOQICPGZGYDT-UHFFFAOYSA-N
Pubchem ID :2735182

Safety of [ 82964-91-8 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314
Precautionary Statements:P280-P305+P351+P338-P310
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 82964-91-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 82964-91-8 ]

[ 82964-91-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 82964-91-8 ]
  • [ 24629-25-2 ]
  • [ 1054529-18-8 ]
  • 2
  • [ 117324-58-0 ]
  • [ 82964-91-8 ]
  • methyl 2-((4-(methylsulfonyl)phenyl)sulfonamido)-5-(trifluoromethyl)benzoate [ No CAS ]
YieldReaction ConditionsOperation in experiment
With indium; In acetonitrile; at 110℃; for 18h; To a solution of <strong>[117324-58-0]methyl 2-amino-5-(trifluoromethyl)benzoate</strong> (0.261 g, 1.19 mmol) and 4-(methylsulfonyl)benzenesulfonyl chloride (0.300 g, 1.18 mmol) in 5 mL acetonitrile was added powdered indium metal (0.027 g, 0.24 mmol). The mixture was stirred at 110 C. for 18 hours. The reaction was then concentrated to a residue. The crude product was purified by silica flash chromatography to afford methyl 2-((4-(methylsulfonyl)phenyl)sulfonamido)-5-(trifluoromethyl)benzoate as a solid. LCMS-ESI- (m/z): [M-H]- calcd 436.01; found 436.18
 

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