Home Cart Sign in  
Chemical Structure| 82514-58-7 Chemical Structure| 82514-58-7

Structure of 82514-58-7

Chemical Structure| 82514-58-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 82514-58-7 ]

CAS No. :82514-58-7
Formula : C6H9ClN2S
M.W : 176.67
SMILES Code : NC1=NC2=C(CCC2)S1.[H]Cl
MDL No. :MFCD00035159

Safety of [ 82514-58-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 82514-58-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 82514-58-7 ]

[ 82514-58-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 82514-58-7 ]
  • [ 53051-97-1 ]
YieldReaction ConditionsOperation in experiment
85% With sodium hydrogencarbonate; In tetrahydrofuran; water; ethyl acetate; at 20℃; for 0.25h; Example 4; 5,6-Dihydro-4H-cyclopentathiazol-2-ylamine (2), free base: The hydrochloride salt of 2 (16.5 g, 93 mmol) (for synthesis of HCl salt, see, e.g., Erlenmeyer and Scheonauer, Helv. Chim. Acta, vol. 24, p. 172E and 175 (1941) and Huenig et al., Chem. Ber., vol. 93, p. 1518-1525 (1960)) was added to a mixture of aqueous sodium bicarbonate (16.5 g, 250 mL) and 25% THF/EtOAc (160 mL, v/v). The mixture was stirred at room temperature for 15 min. The mixture was clarified by filtration through a pad of celite. The organic layer was separated, dried (MgSO4), and concentrated in vacuo to 47 g. Toluene (100 mL) was added and the mixture was concentrated in vacuo to 45 g. The mixture was diluted with heptane (40 mL), cooled, and the product was collected by filtration and dried to give the title compound as the free base (10.75 g, 85%). 1H NMR (CD3OD) delta 4.88 (2H, s), 2.75-2.70 (2H, m), 2.60-2.55 (2H, m), 2.39-2.33 (2H, m).
 

Historical Records

Technical Information

Categories