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Chemical Structure| 779328-99-3 Chemical Structure| 779328-99-3

Structure of 779328-99-3

Chemical Structure| 779328-99-3

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Product Details of [ 779328-99-3 ]

CAS No. :779328-99-3
Formula : C12H14BrClO3
M.W : 321.59
SMILES Code : O=C(OC(C)(C)C)COC1=CC=C(Cl)C=C1Br
MDL No. :MFCD22575908

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Application In Synthesis of [ 779328-99-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 779328-99-3 ]

[ 779328-99-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 779328-99-3 ]
  • [ 145349-76-4 ]
  • [ 779329-00-9 ]
YieldReaction ConditionsOperation in experiment
With cesium fluoride;(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; for 3.0h;Heating / reflux; A mixture of the product from step (i) (2G), 4- (ETHYLTHIO) PHENYLBORONIC ACID (1. 5G), cesium fluoride (2g) and Pd (DPPF) CL2 (0.2g) in dioxane (40ml) was heated under reflux for 3h. After cooling the mixture was partitioned between diethylether and water. The organics were separated, dried and evaporated under reduced pressure. The residue was purified by chromatography on silica ELUTING WITH 5% ETOAC/ISO-HEXANE. YIELD 0.92g MS: APCI (+ve): 379/381 (M+1)
 

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