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[ CAS No. 771-97-1 ]

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Chemical Structure| 771-97-1
Chemical Structure| 771-97-1
Structure of 771-97-1 * Storage: {[proInfo.prStorage]}

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Product Details of [ 771-97-1 ]

CAS No. :771-97-1 MDL No. :MFCD00004116
Formula : C10H10N2 Boiling Point : -
Linear Structure Formula :- InChI Key :N/A
M.W :158.20 g/mol Pubchem ID :69872
Synonyms :

Safety of [ 771-97-1 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 771-97-1 ]

  • Upstream synthesis route of [ 771-97-1 ]
  • Downstream synthetic route of [ 771-97-1 ]

[ 771-97-1 ] Synthesis Path-Upstream   1~10

  • 1
  • [ 2050-75-1 ]
  • [ 771-97-1 ]
YieldReaction ConditionsOperation in experiment
75% With hydrogenchloride; ammonia; ammonium chloride In ethanol for 6 h; Reflux Compound 1 (2 gm) was dissolved in absolute ethanol. Ammonium chloride (1.5 gm),dil. HCl (in catalytic amount) and excess of strong ammonium solution were added to it and reuxed for 6 h on water bath till appearing of permanent dark greenish colour. After completion of reaction, solution was cooled and kept in deep freezer for overnight. Greenish crystals were fltered, dried and recrystallized with methanol. Dark greenish crystals;Yield 75percent; Rf 0.89, Rf 0.82; mp 150 °C; IR (νmax,KBr, cm-1): 758, 854, 1473 (aromatic =C-N), 1500(aromatic C=C), 1681 (N-H), 3049 (N-H); 1H-NMR(CDCl3 500 MHz): 7.45-7.46 (dd, J=3.5-4 Hz, 2H,Ar-H), 7.12-7.14 (dd, J=3-3.5 Hz, 2H, Ar-H), 7.09 (s,Ar-H, 2H), 7.05 (s, Ar-NH2,4H).
Reference: [1] Oriental Journal of Chemistry, 2017, vol. 33, # 2, p. 821 - 828
  • 2
  • [ 92-44-4 ]
  • [ 771-97-1 ]
Reference: [1] Chemische Berichte, 1894, vol. 27, p. 764
[2] Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 3, p. 496
[3] Journal of the Chemical Society, 1910, vol. 97, p. 1716
[4] Oriental Journal of Chemistry, 2017, vol. 33, # 2, p. 821 - 828
  • 3
  • [ 5417-63-0 ]
  • [ 771-97-1 ]
Reference: [1] Helvetica Chimica Acta, 1937, vol. 20, p. 520,524
  • 4
  • [ 91-59-8 ]
  • [ 771-97-1 ]
Reference: [1] Chemische Berichte, 1906, vol. 39, p. 3021[2] Chem. Zentralbl., 1907, vol. 78, # I, p. 1651
  • 5
  • [ 91-59-8 ]
  • [ 771-97-1 ]
  • [ 2243-63-2 ]
Reference: [1] Chemische Berichte, 1906, vol. 39, p. 3021[2] Chem. Zentralbl., 1907, vol. 78, # I, p. 1651
  • 6
  • [ 13115-28-1 ]
  • [ 771-97-1 ]
Reference: [1] Chemistry and Industry (London, United Kingdom), 1954, p. 1174
[2] Bulletin de la Societe Chimique de France, 1972, p. 1551 - 1561
  • 7
  • [ 532-02-5 ]
  • [ 771-97-1 ]
Reference: [1] Chemische Berichte, 1906, vol. 39, p. 3021[2] Chem. Zentralbl., 1907, vol. 78, # I, p. 1651
[3] Chemische Berichte, 1906, vol. 39, p. 3021[4] Chem. Zentralbl., 1907, vol. 78, # I, p. 1651
  • 8
  • [ 29492-74-8 ]
  • [ 771-97-1 ]
Reference: [1] Chemistry and Industry (London, United Kingdom), 1954, p. 1174
  • 9
  • [ 92-44-4 ]
  • [ 771-97-1 ]
Reference: [1] Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 3, p. 496
[2] Chemische Berichte, 1894, vol. 27, p. 763
  • 10
  • [ 91-20-3 ]
  • [ 91-59-8 ]
  • [ 771-97-1 ]
  • [ 2243-63-2 ]
Reference: [1] Chemische Berichte, 1906, vol. 39, p. 3021[2] Chem. Zentralbl., 1907, vol. 78, # I, p. 1651
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