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Chemical Structure| 760212-55-3 Chemical Structure| 760212-55-3

Structure of 760212-55-3

Chemical Structure| 760212-55-3

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Product Details of [ 760212-55-3 ]

CAS No. :760212-55-3
Formula : C19H13BrN2
M.W : 349.22
SMILES Code : BrC1=CC=C2N(C3=CC=CC=C3)C(C4=CC=CC=C4)=NC2=C1
MDL No. :MFCD28129445

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Application In Synthesis of [ 760212-55-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 760212-55-3 ]

[ 760212-55-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 760212-55-3 ]
  • [ 867044-28-8 ]
  • 1,2-diphenyl-5-[9,10-di(2-naphthyl)anthracen-2-yl]-1H-benzimidazole [ No CAS ]
YieldReaction ConditionsOperation in experiment
61% With sodium carbonate;tetrakis(triphenylphosphine) palladium(0); In 1,2-dimethoxyethane; water; for 8h;Heating / reflux; 1.7 g (4.9 mmol) of 5-bromo-1,2-diphenyl-1H-benzimidazole, 2.5 g (5.3 mmol) of 9,10-di(2-naphtyl)anthracene-2-boronic acid, and 0.11 g (0.097 mmol) of tetrakis(triphenylphosphine)palladium were dissolved into 20 mL of 1,2-dimethoxyethane. Then, 10 mL of a 2 M aqueous solution of sodium carbonate were added, and the whole was refluxed under heating for 8 hours in an argon atmosphere. After the completion of the reaction, the resultant was filtered, and the resultant solid was washed with water, methanol, and toluene to obtain 2.1 g of a greenish white solid (61% yield). Mass spectral analysis confirmed that the solid was a target product. The solid had an m/e of 698 with respect to a molecular weight of 698.27.
 

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