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Chemical Structure| 7523-34-4 Chemical Structure| 7523-34-4

Structure of 7523-34-4

Chemical Structure| 7523-34-4

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Product Details of [ 7523-34-4 ]

CAS No. :7523-34-4
Formula : C11H12ClNO
M.W : 209.67
SMILES Code : OC1=CC=C2C=CC=CC2=C1CN.[H]Cl
MDL No. :MFCD01444633

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Application In Synthesis of [ 7523-34-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7523-34-4 ]

[ 7523-34-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 3382-18-1 ]
  • [ 7523-34-4 ]
  • [ 23062-88-6 ]
YieldReaction ConditionsOperation in experiment
73% With triethylamine; In 1,4-dioxane; at 100℃; for 1.5h;Microwave irradiation; General procedure: The mixture of the appropriate aminonaphtholhydrochloride (0.44mmol), 6,7-dimethoxy-3,4-dihydroisoquinoline (2a, 0.4mmol) or 3,4-dihydroisoquinoline (2b, 0.4mmol) and Et3N (60mg, 0.6mmol) in 1,4-dioxane (5mL) was placed in a 10mL reaction vial and heated in a CEM LabMate microwave reactor under the microwave conditions given depicted in Tables 1 and 2. The solvent was then evaporated off and the crude product was crystallized with cold EtOH (8-12mL), filtered off and recrystallized from EtOH (11-15mL).
 

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