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Chemical Structure| 729-17-9 Chemical Structure| 729-17-9

Structure of 729-17-9

Chemical Structure| 729-17-9

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Product Details of [ 729-17-9 ]

CAS No. :729-17-9
Formula : C15H14O3
M.W : 242.27
SMILES Code : O=C(C1=CC=C(C2=CC=C(OC)C=C2)C=C1)OC
MDL No. :MFCD01122234

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Application In Synthesis of [ 729-17-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 729-17-9 ]

[ 729-17-9 ] Synthesis Path-Downstream   1~3

  • 2
  • [ 729-17-9 ]
  • [ 725-14-4 ]
YieldReaction ConditionsOperation in experiment
98% [0158] Step 2 : 4 -METHOXY-BIPHENYL-4-CARBOXYLIC acid. 1 N NAOH (148.5 mL, 148. 5 mmol) was added under nitrogen to a solution of 4 -METHOXY-BIPHENYL-4-CARBOXYLIC acid methyl ester (12. 0G, 49.5 mmol), prepared in the previous step, in 1 L of THF plus 250 ML of water at room temperature. After the addition the reaction was refluxed for 16.5 h (overnight). After cooling to approximately room temperature the reaction was acidified by the addition of 1 N HC1 and then concentrated under reduced pressure. The solid that formed was collected by filtration and dried under reduced pressure to give 4 -METHOXY-BIPHENYL-4-CARBOXYLIC acid (11. 11 G, 98%) as a white solid, mp 245-250C ; MS (ESI) M/Z 227 [M-H]-. Elemental Analysis for C14H1203 : Calc'd: C, 73.67 ; H, 5.30 ; N, 0.00 ; Found: C, 69.52 ; H, 5.01 ; N, 0.04.
  • 3
  • [ 104-92-7 ]
  • [ 1126-46-1 ]
  • [ 792-74-5 ]
  • [ 729-17-9 ]
 

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