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Chemical Structure| 71516-48-8 Chemical Structure| 71516-48-8

Structure of 71516-48-8

Chemical Structure| 71516-48-8

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Product Details of [ 71516-48-8 ]

CAS No. :71516-48-8
Formula : C11H14O3
M.W : 194.23
SMILES Code : C1(COCC2=CC=CC=C2)OCCO1

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Application In Synthesis of [ 71516-48-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 71516-48-8 ]

[ 71516-48-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 71516-48-8 ]
  • [ 5694-68-8 ]
YieldReaction ConditionsOperation in experiment
97.3% With hydrogen;palladium(II) hydroxide/carbon; In methanol; at 20℃; for 15h; (66b) 1,3-dioxolan-2-ylmethanol To a methanol (100 ml) solution of 2-((benzyloxy)methyl)-1,3-dioxolane (3.01 g, 15.5 mmol) obtained in the step (66a) above, palladium hydroxide (20 wt. percent Pd (dry basis) on carbon, wet (water max. 50percent))(300 mg) was added and the mixture was stirred in a hydrogen atmosphere at room temperature for 15 hours. The reaction vessel was purged with nitrogen and a catalyst was removed by filtration through celite, and then, washed with methanol. The filtrate was concentrated and dried under reduced pressure to obtain the title compound (1.57 g, 97.3percent yield) as a light yellow oil. 1H NMR(400 MHz, CDCl3) deltappm; 1.89(1H, br s), 3.66-3.72(2H, m), 3.88-4.08(4H, m), 5.01(1H, t, J=3 Hz).
  • 2
  • [ 5694-68-8 ]
  • [ 100-39-0 ]
  • [ 71516-48-8 ]
 

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