7149-14-6|3-Bromo-4-iodonitrobenzene| Ambeed

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Quality Control of [ 7149-14-6 ] Purity: 98% SDS Specification

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Product Details of [ 7149-14-6 ]

CAS No. :	7149-14-6
Formula :	C₆H₃BrINO₂
M.W :	327.90
SMILES Code :	O=[N+](C1=CC=C(I)C(Br)=C1)[O-]
MDL No. :	MFCD09878135
InChI Key :	CJUZKENURNQSDJ-UHFFFAOYSA-N
Pubchem ID :	238706

Safety of [ 7149-14-6 ]

GHS Pictogram:
Signal Word:	Warning
Hazard Statements:	H302-H315-H319-H335
Precautionary Statements:	P261-P301+P312-P302+P352-P304+P340-P305+P351+P338

Application In Synthesis of [ 7149-14-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 7149-14-6 ]

[ 7149-14-6 ] Synthesis Path-Downstream 1~35

1
[ 13296-94-1 ]
[ 7149-14-6 ]

Yield	Reaction Conditions	Operation in experiment
77%	With potassium iodide; sodium nitrite; In water; acetonitrile; at 0 - 5℃; for 0.5h;	Ice-cold solution of sodium nitrite (57.2 g, 829 mmol) and potassium iodide (138 g, 829 mmol) in water (25 mL) was added drop wise simultaneously to a stirred suspension of 2-bromo-4-nitroaniline (60 g, 276 mmol) in acetonitrile (250 mL) at 0-5 C and stirred for 30 minutes. The reaction mixture was then poured on to ice-cold water (1000 mL). The solid obtained was filtered, washed with water and dried to afford the titlecompound.Yield: 70.0 g (77 %); 1H NMR (300 MHz, CDCI3): O 7.86 (dd, 1H, J= 8.7, 2.4 Hz, Ar), 8.10(d, 1H, J= 8.7 Hz, Ar), 8.45 (d, 1H, J= 2.4 Hz, Ar); MS (El, 70 eV): m/z 328.3 (M+H).

References: [1]Patent: WO2015/49629,2015,A1 .Location in patent: Page/Page column 102.
[2]Gazzetta Chimica Italiana,1874,vol. 4,p. 341.
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften,1875,p. 317.
[3]Chemistry - A European Journal,2017,vol. 23,p. 2660 - 2665.

2
[ 7149-14-6 ]
[ 105837-74-9 ]

References: [1]Zhurnal Obshchei Khimii,1956,vol. 26,p. 2524,2528; engl. Ausg. S. 2817, 2820.

3
[ 7149-14-6 ]
[ 72342-73-5 ]

References: [1]Journal of the Indian Chemical Society,1963,vol. 40,p. 979.

5
[ 7149-14-6 ]
[ 7664-41-7 ]
[ 13296-94-1 ]

References: [1]Gazzetta Chimica Italiana,1874,vol. 4,p. 341.
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften,1875,p. 317.

6
o-bromo-iodobenzene [ No CAS ]
[ 7149-14-6 ]

References: [1]Gazzetta Chimica Italiana,1874,vol. 4,p. 341.
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften,1875,p. 317.

7
[ 5720-07-0 ]
[ 7149-14-6 ]
2-bromo-4'-methoxy-4-nitrobiphenyl [ No CAS ]