70931-33-8|1-(4-Fluorophenethyl)piperazine| Ambeed

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Quality Control of [ 70931-33-8 ] Purity: 97% SDS Specification

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Product Details of [ 70931-33-8 ]

CAS No. :	70931-33-8
Formula :	C₁₂H₁₇FN₂
M.W :	208.28
SMILES Code :	FC1=CC=C(CCN2CCNCC2)C=C1
MDL No. :	MFCD09839701
InChI Key :	LODHVDKKTUZVDK-UHFFFAOYSA-N
Pubchem ID :	11254522

Safety of [ 70931-33-8 ]

GHS Pictogram:
Signal Word:	Warning
Hazard Statements:	H302-H315-H319-H335
Precautionary Statements:	P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 70931-33-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 70931-33-8 ]

[ 70931-33-8 ] Synthesis Path-Downstream 1~35

1
[ 56097-05-3 ]
[ 70931-33-8 ]
3-(8-Chloro-3-fluoro-10,11-dihydro-dibenzo[b,f]thiepin-10-yl)-1-[2-(4-fluoro-phenyl)-ethyl]-piperazine [ No CAS ]

References: [1]Collection of Czechoslovak Chemical Communications,1981,vol. 46,p. 141 - 147.

2
[ 61150-65-0 ]
[ 70931-33-8 ]
3-(8-Chloro-3,7-difluoro-10,11-dihydro-dibenzo[b,f]thiepin-10-yl)-1-[2-(4-fluoro-phenyl)-ethyl]-piperazine [ No CAS ]

References: [1]Collection of Czechoslovak Chemical Communications,1981,vol. 46,p. 141 - 147.

3
[ 70931-36-1 ]
[ 70931-33-8 ]

Yield	Reaction Conditions	Operation in experiment
	With potassium hydroxide; In ethanol; water; toluene;	37.2 g of 1-ethoxycarbonyl-4-[2-(4-fluorophenyl)ethyl]-piperazine are dissolved in 55 ml of ethanol, and a solution of 47 g of potassium hydroxide in 12.5 ml of water is added dropwise, while stirring. The whole is heated at 115-120 for 6 hours while stirring, concentrated to dryness by evaporation, taken up in toluene, washed with saturated sodium chloride solution and concentrated to dryness by evaporation under reduced pressure. The 1-[2-(4-fluorophenyl)ethyl]-piperazine which remains behind can be purified via the dihydrochloride which has a melting point of 270-272.

References: [1]Collection of Czechoslovak Chemical Communications,1980,vol. 45,p. 3182 - 3189.
[2]Patent: US4804661,1989,A .

4
[ 70931-33-8 ]
[ 70931-13-4 ]
[ 70931-34-9 ]

References: [1]Collection of Czechoslovak Chemical Communications,1987,vol. 52,p. 1811 - 1833.

5
[ 70931-33-8 ]
[ 13459-65-9 ]
[ 77602-97-2 ]

References: [1]Collection of Czechoslovak Chemical Communications,1980,vol. 45,p. 3182 - 3189.

6
[ 70931-33-8 ]
[ 191351-60-7 ]
4-[2-(4-fluorophenyl)ethyl]-1-[2-fluoro-3-(5-(1,2,4-triazol-4-yl)-1H-indol-3-yl)propyl]piperazine [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1999,vol. 42,p. 2087 - 2104.

7
[ 109-09-1 ]
[ 70931-33-8 ]
1-[2-(4-fluoro-phenyl)-ethyl]-4-pyridin-2-yl-piperazine [ No CAS ]