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Chemical Structure| 7003-32-9 Chemical Structure| 7003-32-9

Structure of 7003-32-9

Chemical Structure| 7003-32-9

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Product Details of [ 7003-32-9 ]

CAS No. :7003-32-9
Formula : C7H15N
M.W : 113.20
SMILES Code : NC1C(C)CCCC1
MDL No. :MFCD00001492
InChI Key :FEUISMYEFPANSS-UHFFFAOYSA-N
Pubchem ID :23432

Safety of [ 7003-32-9 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H225-H302-H314
Precautionary Statements:P280-P305+P351+P338-P310
Class:8(3)
UN#:2734
Packing Group:

Application In Synthesis of [ 7003-32-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7003-32-9 ]

[ 7003-32-9 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 63176-44-3 ]
  • [ 7003-32-9 ]
  • 2-methyl-N-(2-methylcyclohexyl)-1H-indole-3-carboxamide [ No CAS ]
  • 3
  • [ 99-14-9 ]
  • [ 7003-32-9 ]
  • 1,2,3-propanetricarboxylic acid tris(2-methylcyclohexylamide) [ No CAS ]
YieldReaction ConditionsOperation in experiment
61% Comparative Example 1 [Synthesis of Thickening/stabilizing Agent (3) (1,2,3-propanetricarboxylic acid tris(2-methylcyclohexylamide))] (0087) A 100 mL four-necked separable flask equipped with a Dimroth condenser, a nitrogen inlet, a dropping funnel and a thermocouple was charged with 20 mL of pyridine, 2.97 g (0.017 mol) of 1,2,3-propanetricarboxylic acid, and 7.0 g (0.056 mol) of diisopropylcarbodiimide, and the resultant was aged for 3 hours with a temperature within the system set to 50 C. (0088) Thereafter, 5.7 g (0.051 mol) of 2-methylcyclohexylamine was added thereto, and the resultant was aged for another 8 hours. (0089) Then, a low-boiling component of the thus obtained crude liquid was removed with an evaporator, and the resultant was washed with methanol to obtain a pale yellow wet powder. The thus obtained wet powder was washed with acetone to obtain 4.7 g of 1,2,3-propanetricarboxylic acid tris(2-methylcyclohexylamide) (yield: 61%).
61% In a 100 mL four-neck separable flask equipped with a Dimroth condenser, a nitrogen inlet, a dropping funnel and a thermocouple, 20 mL of pyridine, 2.97 g (0.017 mol) of 1, 2, 3-propane tricarboxylic acid, 7.0 g of diisopropyl carbo diimide (0.056 mol) were charged, and the temperature in the system was set at 50 C and aged for 3 hours. Further, 5.7 g (0.051 mol) of 2-methyl cyclohexyl amine was charged and aged for 8 hours. Thereafter, the low boiling fraction of the resulting crude liquid was removed by an evaporator and washed with methanol to obtain light yellow wet powder. Further, the obtained wet powder was washed with acetone to obtain 4.7 g of 1, 2, 3-propane tricarboxylic acid tris (2-methyl cyclohexyl amide) (yield: 61%).
 

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