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Chemical Structure| 69026-14-8 Chemical Structure| 69026-14-8

Structure of 69026-14-8

Chemical Structure| 69026-14-8

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Product Details of [ 69026-14-8 ]

CAS No. :69026-14-8
Formula : C14H12O3
M.W : 228.24
SMILES Code : O=C(O)C1=CC=CC(OCC2=CC=CC=C2)=C1
MDL No. :MFCD00527901
InChI Key :CISXCTKEQYOZAM-UHFFFAOYSA-N
Pubchem ID :309226

Safety of [ 69026-14-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 69026-14-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 69026-14-8 ]

[ 69026-14-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 79-37-8 ]
  • [ 29608-05-7 ]
  • [ 69026-14-8 ]
  • 3-benzoyloxy-4'-(piperidinomethyl)benzanilide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With sodium chloride; triethylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide; Example 84 (Production of Compound 84) To 3-benzyloxybenzoic acid (800 mg) dissolved in THF (10 ml) were added oxalyl chloride (397 mul) and one drop of DMF, and the resulting mixture was stirred at room temperature for one hour. After the reaction mixture was evaporated to remove the solvent, to the residue dissolved in THF (15 ml) were added dropwise at room temperature <strong>[29608-05-7]1-(4-aminobenzyl)piperidine</strong> (733 mg) and triethylamine (589 mul). This reaction mixture was stirred at room temperature for 17 hours, was then mixed with water (100 ml) and was extracted with ethyl acetate. The organic layer was washed with an aqueous saturated solution of sodium chloride, was dried with anhydrous sodium sulfate and was then evaporated under reduced pressure to remove the solvent. The resulting residue was recrystallized from ethyl acetate/hexane to obtain 3-benzyloxy-4'-(piperidinomethyl)benzanilide (compound 84) (1.06 g) as colorless crystals.
  • 2
  • [ 29608-05-7 ]
  • [ 69026-14-8 ]
  • 3-benzoyloxy-4'-(piperidinomethyl)benzanilide [ No CAS ]
 

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