Alternatived Products of [ 6848-73-3 ] Product Details of [ 6848-73-3 ]
CAS No. : | 6848-73-3 | MDL No. : | MFCD11499064 |
Formula : |
C10H14O3 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | - |
M.W : |
182.22
| Pubchem ID : | - |
Synonyms : | |
Application In Synthesis of [ 6848-73-3 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 6848-73-3 ]
- 1
- [ 6848-73-3 ]
- [ 38480-94-3 ]
Yield | Reaction Conditions | Operation in experiment |
65% | With potassium dichromate; sulfuric acid; In water; | 18F 2',3'-Dimethoxyacetophenone A solution of potassium dichromate (24.76 g), water (124 ml) and concentrated sulfuric acid (12 ml) was added with 2-(2,3-dimethoxyphenyl)ethan-2-ol (10.06 g, 55.3 mmol) and left under stirring at room temperature for 15 min. After that the mixture was extracted with ethyl ether and washed successively with a 5percent potassium carbonate solution (2*150 ml) and with a sodium chloride saturated solution (1*100 ml). The solvent was dried and evaporated under reduced pressure to obtain a residue which was purified by distillation under high vacuum. At a pressure of 0.3 torr and at a temperature of 85° C., 6.47 g of the title compound distiled (65percent yield). 1 H N.M.R. (300 MHz, CDCl3) delta ppm: 2.62 (s, 3H); 3.88 (s, 3H); 3.90 (s, 3H); 7.05-7.10 (sc, 2H); 7.21 (dd, 1H). |
Reference: [1]Patent: US5990142,1999,A [2]Journal of the American Chemical Society,1951,vol. 73,p. 793 [3]Chemische Berichte,1913,vol. 46,p. 4019 [4]Journal of the American Chemical Society,2005,vol. 127,p. 10371 - 10387 - 2
- [ 6848-73-3 ]
- diluted Cr2O3-H2SO4 [ No CAS ]
- [ 38480-94-3 ]
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