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Chemical Structure| 65055-17-6 Chemical Structure| 65055-17-6

Structure of 65055-17-6

Chemical Structure| 65055-17-6

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Product Details of [ 65055-17-6 ]

CAS No. :65055-17-6
Formula : C7H3Cl2FO
M.W : 193.00
SMILES Code : O=C(Cl)C1=CC=C(F)C(Cl)=C1
MDL No. :MFCD00236215
InChI Key :DLZUHSFUBZTBQZ-UHFFFAOYSA-N
Pubchem ID :2736548

Safety of [ 65055-17-6 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314-H290
Precautionary Statements:P501-P234-P264-P280-P390-P303+P361+P353-P301+P330+P331-P363-P304+P340+P310-P305+P351+P338+P310-P406-P405
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 65055-17-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 65055-17-6 ]

[ 65055-17-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 67-56-1 ]
  • [ 65055-17-6 ]
  • [ 234082-35-0 ]
YieldReaction ConditionsOperation in experiment
97.29% In methanol; at 60℃; for 1h; Example 1 Preparation of methyl 3-chloro-4-fluoro-benzoate In a 250 ml four-necked round bottom flask, equipped with a mechanical stirrer, condenser and thermometer, 86.5 g of 3-chloro-4-fluoro-benzoic acid chloride are loaded and 28.1 g of anhydrous MeOH are added by a dosing funnel. The reaction is exothermic and spontaneously reaches 60C. The methanol is metered keeping the temperature at about 60. It is stirred for 1 hour then the excess methanol is distilled. In this way 80 g of yellow oil are obtained corresponding to the compound methyl 3-chloro-4-fluoro-benzoate. Yield 97.29%.
 

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