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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 64688-68-2 Chemical Structure| 64688-68-2

Structure of 64688-68-2

Chemical Structure| 64688-68-2

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Product Details of [ 64688-68-2 ]

CAS No. :64688-68-2
Formula : C8H6ClNO3
M.W : 199.59
SMILES Code : O=C(Cl)C1=CC([N+]([O-])=O)=CC=C1C
MDL No. :MFCD03701211

Safety of [ 64688-68-2 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301-H311-H314-H331
Precautionary Statements:P260-P264-P280-P301+P330+P331+P310-P303+P361+P353+P310+P363-P304+P340+P310-P305+P351+P338+P310-P405-P501
Class:6.1(8)
UN#:2928
Packing Group:

Application In Synthesis of [ 64688-68-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 64688-68-2 ]

[ 64688-68-2 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 939-83-3 ]
  • [ 64688-68-2 ]
  • 2
  • [ 64688-68-2 ]
  • [ 66521-66-2 ]
  • [ 1436405-97-8 ]
YieldReaction ConditionsOperation in experiment
51% With pyridine; at 0 - 20℃; for 3h; General procedure: Commercially available 4-(pyridin-3-yl) pyrimidin-2-amine 57 (0.3 g, 1.74 mmol) was added to the solution of 56 (0.38 g, 2 mmol) in pyridine (8 mL) at 0 °C and stirred at room temperature for 3 h. The reaction solution was diluted with water (50 mL) and the resulting solid was filtered, washed with water, and dried to give 4-ethoxy-3-nitro-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzamide 58c (0.31 g, 51percent) as a light-brown solid. 1H NMR (DMSO-d6, delta): 1.37(t, 3H), 4.32(q, 2H), 7.50(d, 1H), 7.75(dd, 1H), 7.99(d, 1H), 8.29(dd, 1H), 8.54(d, 1H), 8.74(d, 1H), 8.83(d, 1H), 8.88(d, 1H), 9.44(d, 1H), 11.33(br, 1H).
  • 3
  • [ 64688-68-2 ]
  • [ 1030825-20-7 ]
 

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