CAS No. : | 6443-69-2 | MDL No. : | MFCD00008397 |
Formula : | C10H14O3 | Boiling Point : | No data available |
Linear Structure Formula : | C6H2CH3(OCH3)3 | InChI Key : | KCIZTNZGSBSSRM-UHFFFAOYSA-N |
M.W : | 182.22 | Pubchem ID : | 80922 |
Synonyms : |
Signal Word: | Warning | Class: | |
Precautionary Statements: | P210-P280-P370+P378-P403+P235-P501 | UN#: | |
Hazard Statements: | H227-H315 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
60% | With zirconium(IV) chloride; methoxybenzene; In dichloromethane; at 60℃; for 24.0h;Sealed tube; | The 91 mg (0.5mmol) 3, 4, 5-trimethoxy toluene, 233 mg zirconium chloride (ZrCl 4) (1mmol), 218 mu L anisole (2mmol) and 3mL1,2-dichloroethane by adding 10 ml in the reaction pipe, sealing, 60 °C reaction under the conditions of 24h. Reaction after the stop, the extraction with ethyl acetate, saturated salt water washing, drying by anhydrous sodium sulfate, filtered, the filtrate is distilled under reduced pressure, purification by the silica gel column column chromatography separation, product 4-methyl -2,6-dimethoxy- phenol approximately 51 mg, yield 60percent. |
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