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Chemical Structure| 6358-64-1 Chemical Structure| 6358-64-1

Structure of 6358-64-1

Chemical Structure| 6358-64-1

2,5-Dimethoxy-4-chloroaniline

CAS No.: 6358-64-1

4.5 *For Research Use Only !

Cat. No.: A973014 Purity: 98%

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Product Details of [ 6358-64-1 ]

CAS No. :6358-64-1
Formula : C8H10ClNO2
M.W : 187.62
SMILES Code : COC1=CC(N)=C(OC)C=C1Cl
MDL No. :MFCD00014893
InChI Key :YGUFQYGSBVXPMC-UHFFFAOYSA-N
Pubchem ID :22833

Safety of [ 6358-64-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302
Precautionary Statements:P280-P305+P351+P338

Application In Synthesis of [ 6358-64-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6358-64-1 ]

[ 6358-64-1 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 92-70-6 ]
  • [ 6358-64-1 ]
  • [ 4273-92-1 ]
YieldReaction ConditionsOperation in experiment
92% In water; chlorobenzene; toluene; at 85℃; for 5h; 1. 1 part of the material 2-hydroxy-3-naphthoic acid (the amount of the substance,The same below) dissolved in water and immiscible solvent 1.1 (such as toluene, chlorobenzene),The solution was added to the reactor (Figure 1),Then, 1.15 parts of 2,5-dimethoxy-4-chloroaniline was added,The reaction mixture was heated at a temperature of 85 C,The reaction time was 5h, and the crude product was obtained in 89% yield.2. Distillation of crude products, the yield of 94%.3. Add the refined product to a separate dryer (Figure 2)The rising steam is evenly contacted with the crude phenol concentrate through the steam distributor,Water vapor cold liquid liquefaction into small water droplets, dissolved products in the soluble impurities,Excessive steam is condensed at the top of the condenser to form a stream of water into the desiccator to rinse the phenolic AS-LC product,After repeated rinsing three times, finally, in the jacket outside the dryer through the water vapor,The dryer was dried by heating to give the final product in a yield of 92%.
  • 2
  • [ 615-67-8 ]
  • [ 6358-64-1 ]
  • 3
  • [ 23094-96-4 ]
  • [ 6358-64-1 ]
  • C22H20Br2ClNO8S2 [ No CAS ]
  • 3-bromo-N-(4-chloro-2,5-dimethoxyphenyl)-4-methoxybenzenesulfonamide [ No CAS ]
  • 4
  • [ 23094-96-4 ]
  • [ 6358-64-1 ]
  • 3-bromo-N-(4-chloro-2,5-dimethoxyphenyl)-4-methoxybenzenesulfonamide [ No CAS ]
 

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