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Chemical Structure| 635698-34-9 Chemical Structure| 635698-34-9

Structure of 635698-34-9

Chemical Structure| 635698-34-9

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Product Details of [ 635698-34-9 ]

CAS No. :635698-34-9
Formula : C13H13N3O2
M.W : 243.26
SMILES Code : O=C1NC(CN(CC2=CC=CC=C2)C3)=C3C(N1)=O
MDL No. :MFCD10699254
InChI Key :HHPFBTNJYIYLKC-UHFFFAOYSA-N
Pubchem ID :37819057

Safety of [ 635698-34-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H332-H335
Precautionary Statements:P261-P280-P305+P351+P338

Application In Synthesis of [ 635698-34-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 635698-34-9 ]

[ 635698-34-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1027-35-6 ]
  • [ 57-13-6 ]
  • [ 635698-34-9 ]
YieldReaction ConditionsOperation in experiment
43% With sodium methylate; In methanol; ethanol; for 24h;Heating / reflux; Ethyl 1-benzyl-4-oxopyrrolidine-3-carboxylate (9.23 g, 0.0372 mol) prepared according to Reference Example 2 was dissolved in ethanol (170 mL), and the solution was mixed with urea (11.2 g, 0.186 mol) and a solution of sodium methoxide in methanol (about 28percent, 25 g), followed by stirring under reflux for twenty-four hours. The reaction mixture was mixed with water (100 mL), followed by stirring at room temperature. Diluted hydrochloric acid (about 1 mol/L, 100 mL) was added dropwise to the reaction mixture. The precipitated crystals were collected by filtration, and the collected crystals were washed with water (100 mL). The crystals were dried under reduced pressure and thereby yielded 6-benzyl-6,7-dihydro-5H-pyrrolo[3,4-d]pyrimidine-2,4(1H,3H)-dione (3.93 g, in a yield of 43percent).
 

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