63134-33-8|4-((4-(Benzyloxy)phenyl)sulfonyl)phenol| Ambeed

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Quality Control of [ 63134-33-8 ] Purity: 98% SDS Specification

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Product Details of [ 63134-33-8 ]

CAS No. :	63134-33-8
Formula :	C₁₉H₁₆O₄S
M.W :	340.39
SMILES Code :	OC1=CC=C(S(=O)(C2=CC=C(OCC3=CC=CC=C3)C=C2)=O)C=C1
MDL No. :	MFCD00185925
InChI Key :	UWPJWCBDMZHMTN-UHFFFAOYSA-N
Pubchem ID :	113063

Safety of [ 63134-33-8 ]

GHS Pictogram:
Signal Word:	Warning
Hazard Statements:	H302+H312+H332-H315-H319
Precautionary Statements:	P261-P264-P270-P271-P280-P301+P312+P330-P302+P352+P312+P362+P364-P304+P340+P312-P305+P351+P338+P337+P313-P501

Application In Synthesis of [ 63134-33-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 63134-33-8 ]

[ 63134-33-8 ] Synthesis Path-Downstream 1~12

1
[ 80-09-1 ]
[ 100-39-0 ]
[ 63134-33-8 ]

Yield	Reaction Conditions	Operation in experiment
16%	With sodium hydroxide; In water; at 80.0℃; for 24.0h;Inert atmosphere;	General procedure: Bisphenol A (20mmol, 4.566g) was added to a 250mL round bottom flask containing NaOH aqueous solution (40mmol, 150mL, 1.599g). The reactor was then equipped with a reflux condenser and brought to 80C in a nitrogen environment with vigorous stirring via a Teflon-coated magnetic stir bar. Once completely dissolved, benzyl bromide (20mmol, 0.342g) was added via syringe. The mixture was allowed to stir for 2h at 80C in a nitrogen environment. After stirring was ceased, a beige precipitate settled out in a clear solution. While still hot, the supernatant was decanted and the crude product washed with water (ca. 80C). The crude product was then dissolved in chloroform, transferred to a separatory funnel, washed w/10% HCl (v/v), and then washed twice with DI H2O. The organic layer was then dried over magnesium sulfate, filtered into a tared receiver flask, and isolated under vacuum as an off-white solid. The compound was then recrystallized twice from hexanes/ethyl acetate to afford a white, crystalline solid (3.80g, 59.7% yield, mp (DSC)=109C).

References: [1]Journal of Fluorine Chemistry,2014,vol. 166,p. 60 - 68.
[2]Journal of the Chemical Society. Perkin Transactions 1 (2001),2001,p. 2796 - 2803.

2
[ 67852-96-4 ]
[ 63134-33-8 ]
[ 392743-68-9 ]