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Chemical Structure| 624-70-4 Chemical Structure| 624-70-4

Structure of 624-70-4

Chemical Structure| 624-70-4

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Product Details of [ 624-70-4 ]

CAS No. :624-70-4
Formula : C2H4ClI
M.W : 190.41
SMILES Code : ICCCl
MDL No. :MFCD00041453
InChI Key :JTWWWQGSFTWWDL-UHFFFAOYSA-N
Pubchem ID :136438

Safety of [ 624-70-4 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H225-H315-H319
Precautionary Statements:P210-P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313
Class:3
UN#:1993
Packing Group:

Application In Synthesis of [ 624-70-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 624-70-4 ]

[ 624-70-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 624-70-4 ]
  • [ 67630-01-7 ]
  • [ 189744-28-3 ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate; In N,N-dimethyl-formamide; at -5 - 5℃; for 12h;Large scale; 1-Chloro-2-iodo-ethane (2.095 kg, 11.0 mol), potassium carbonate (1.589 kg, 11.5 mol), N,N-dimethylformamide (5 L) in a 50 L glass kettle, Cool down to -5C, start dropping the mother liquor (13L, 5mol) from step (a), control the temperature at -5C to 5C, and react for 12 hours after the addition is complete.96.7% of the main peak of the sample was detected, and <strong>[67630-01-7]N-tert-butoxycarbonyl-L-4-aminophenylalanine ethyl ester</strong> was not detected. The largest single impurity was 1.43%.Concentrate to remove unreacted 1-chloro-2-iodo-ethane and most of the N,N-dimethylformamide, leaving a volume of about 2L.
 

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