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Chemical Structure| 61058-75-1 Chemical Structure| 61058-75-1

Structure of 61058-75-1

Chemical Structure| 61058-75-1

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Product Details of [ 61058-75-1 ]

CAS No. :61058-75-1
Formula : C12H22O3
M.W : 214.30
SMILES Code : CCCCCCCCCC(CC(O)=O)=O

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Application In Synthesis of [ 61058-75-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 61058-75-1 ]

[ 61058-75-1 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 67342-99-8 ]
  • [ 61058-75-1 ]
YieldReaction ConditionsOperation in experiment
72% With water; sodium hydroxide; In ethanol; at 20℃; for 12h; Compound 12-1 (647 mg, 2.67 mmol, 1 eq.) was dissolved in EtOH/H20 (10/10 mE), then added NaOH (139 mg, 3.47 mmol, 1.3 eq.). The reaction was stirred at 20 C. for 12 h. The reaction mixture was washed twice with ethyl acetate (10 mE). The aqueous layer was adjusted to acidic (pH 3-5) with iN HC1. A white solid was precipitated, filtered and dried in vacuo to obtain compound 13-1 (white solid, 410 mg, 72%). ?H NMR (300 MHz, DMSO) oe 12.53 (s, 1H), 3.43 (s, 2H), 2.39 (t, J=7.2 Hz, 2H), 1.23 (m, 14H), 0.85 (t, J=6.3 Hz, 3H).
 

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