Home Cart Sign in  
Chemical Structure| 608-22-0 Chemical Structure| 608-22-0
Chemical Structure| 608-22-0

2,3-Dibromoaniline

CAS No.: 608-22-0

4.5 *For Research Use Only !

Cat. No.: A555091 Purity: 95%

Change View

Size Price

US Stock

Global Stock

In Stock
250mg łÍÇî¶ÊÊ Inquiry Inquiry

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 250mg

    łÍÇî¶ÊÊ

In Stock

- +

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support Online Technical Q&A
Product Citations

Alternative Products

Product Details of [ 608-22-0 ]

CAS No. :608-22-0
Formula : C6H5Br2N
M.W : 250.92
SMILES Code : NC1=CC=CC(Br)=C1Br
MDL No. :MFCD13185488

Safety of [ 608-22-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313

Application In Synthesis of [ 608-22-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 608-22-0 ]

[ 608-22-0 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 608-22-0 ]
  • [ 823-54-1 ]
  • [ 615-55-4 ]
  • [ 642-95-5 ]
  • 2,3-dibromo-4-chloroaniline [ No CAS ]
  • [ 591-19-5 ]
  • 2
  • [ 591-19-5 ]
  • [ 823-54-1 ]
  • [ 615-55-4 ]
  • [ 608-22-0 ]
  • 3
  • [ 5411-50-7 ]
  • [ 26429-41-4 ]
  • [ 615-55-4 ]
  • [ 608-22-0 ]
YieldReaction ConditionsOperation in experiment
13.7% Example 21 2,3-dibromoaniline: Ref: J. Org. Chem. 1990, 55(9) 2736-2742; Tetrahedron Lett., 1984, 25, 839-42. 1,2-Dibromobenzene (5.0 g, 21.2 mmol) was cooled in an ice bath and treated dropwise with fuming nitric acid (9.75 mL). The mixture was stirred vigorously for 15 minutes and then pipetted portionwise into a flask of crushed ice. The pale yellow solid was removed by filtration, washed with water and air dried to yield 7.613 g of a mixture of regioisomers. The crude material (0.666 g, 2.37 mmol) was dissolved in ethanol (14 mL) and treated with tin(II) chloride hydrate. The solution was refluxed for 1 h and poured into ice water and the pH was adjusted to 9 with 2N NaOH. The mixture was extracted with ether (2*25 mL). The organic extracts were washed with saturated sodium chloride, dried over magnesium sulfate, filtered and concentrated under reduced pressure to yield 0.544 g of crude material as a mixture of regioisomers.
  • 4
  • [ 591-19-5 ]
  • [ 3638-73-1 ]
  • [ 615-55-4 ]
  • [ 608-22-0 ]
 

Historical Records

Technical Information

Categories