Home Cart Sign in  
Chemical Structure| 608-22-0 Chemical Structure| 608-22-0

Structure of 608-22-0

Chemical Structure| 608-22-0

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 608-22-0 ]

CAS No. :608-22-0
Formula : C6H5Br2N
M.W : 250.92
SMILES Code : NC1=CC=CC(Br)=C1Br
MDL No. :MFCD13185488

Safety of [ 608-22-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313

Application In Synthesis of [ 608-22-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 608-22-0 ]

[ 608-22-0 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 608-22-0 ]
  • [ 823-54-1 ]
  • [ 615-55-4 ]
  • [ 642-95-5 ]
  • 2,3-dibromo-4-chloroaniline [ No CAS ]
  • [ 591-19-5 ]
  • 2
  • [ 591-19-5 ]
  • [ 823-54-1 ]
  • [ 615-55-4 ]
  • [ 608-22-0 ]
  • 3
  • [ 5411-50-7 ]
  • [ 26429-41-4 ]
  • [ 615-55-4 ]
  • [ 608-22-0 ]
YieldReaction ConditionsOperation in experiment
13.7% Example 21 2,3-dibromoaniline: Ref: J. Org. Chem. 1990, 55(9) 2736-2742; Tetrahedron Lett., 1984, 25, 839-42. 1,2-Dibromobenzene (5.0 g, 21.2 mmol) was cooled in an ice bath and treated dropwise with fuming nitric acid (9.75 mL). The mixture was stirred vigorously for 15 minutes and then pipetted portionwise into a flask of crushed ice. The pale yellow solid was removed by filtration, washed with water and air dried to yield 7.613 g of a mixture of regioisomers. The crude material (0.666 g, 2.37 mmol) was dissolved in ethanol (14 mL) and treated with tin(II) chloride hydrate. The solution was refluxed for 1 h and poured into ice water and the pH was adjusted to 9 with 2N NaOH. The mixture was extracted with ether (2*25 mL). The organic extracts were washed with saturated sodium chloride, dried over magnesium sulfate, filtered and concentrated under reduced pressure to yield 0.544 g of crude material as a mixture of regioisomers.
  • 4
  • [ 591-19-5 ]
  • [ 3638-73-1 ]
  • [ 615-55-4 ]
  • [ 608-22-0 ]
 

Historical Records

Technical Information

Categories