Home Cart Sign in  
HazMat Fee +

There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.

Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic USD 100+
Accessible (Haz class 3, 4, 5 or 8), International USD 200+
Chemical Structure| 60638-81-5 Chemical Structure| 60638-81-5

Structure of 60638-81-5

Chemical Structure| 60638-81-5

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 60638-81-5 ]

CAS No. :60638-81-5
Formula : C8H7ClO5S
M.W : 250.66
SMILES Code : O=C(OC)C1=CC(S(=O)(Cl)=O)=CC=C1O
MDL No. :MFCD11857789
InChI Key :JCUQSWVHGVRETC-UHFFFAOYSA-N
Pubchem ID :12581955

Safety of [ 60638-81-5 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314
Precautionary Statements:P260-P280-P303+P361+P353-P301+P330+P331-P304+P340+P310-P305+P351+P338+P310
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 60638-81-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 60638-81-5 ]

[ 60638-81-5 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 23069-99-0 ]
  • [ 60638-81-5 ]
  • [ 699016-47-2 ]
YieldReaction ConditionsOperation in experiment
Under nitrogen at room temperature, to a mixture of (2-phenylethyl)formamide (500 mg) and methyl 5-(chlorosulfonyl)-2-hydroxybenzoate (840 mg) in nitrobenzene (5 ml) was added aluminum chloride (1.56 g), and the mixture was stirred at 100 C. for 4 hours.To the resulting mixture were added ice-cold 1N hydrochloric acid and ethyl acetate, and the mixture was stirred for 20 minutes.After separation, the organic layer was dried over anhydrous magnesium sulfate and evaporated under reduced pressure.To the residue was added hydrogen chloride methanol reagent 10 (5 ml) at room temperature under nitrogen, and the mixture was stirred at 40 C. for 2.5 hours.The resulting mixture was evaporated under reduced pressure.To the residue was added diisopropyl ether (20 ml), and the mixture was stirred for 1 hour.The precipitates were collected by filtration and dried in vacuo to give methyl 5-[[4-(2-aminoethyl)-phenyl]sulfonyl]-2-hydroxybenzoate hydrochloride (1.03 g). (+)ESI-MS (m/z): 336 (M-HCl+H)+
  • 2
  • [ 23069-99-0 ]
  • [ 60638-81-5 ]
  • C17H17NO6S [ No CAS ]
YieldReaction ConditionsOperation in experiment
aluminum (III) chloride; In 1,2-dichloro-benzene; at 20 - 80℃; for 3.5h; Preparation 2 To a solution of (2-phenylethyl)formamide.(500 mg) and methyl 5-(chlorosulfonyl)-2-hydroxybenzoate (840' mg) in 1,2- dichlorobenzene (5 ml) was added aluminum chloride (1.56 g) by portions at room temperature under nitrogen, and the mixture was stirred at 80C for 3.5 hours. The resulting mixture was cooled to room temperature, and to this one were added ice, ethyl acetate and 1N hydrochloric acid. After being stirred for 40 minutes, followed by separation, the organic layer was washed successively with water and brine, dried over anhydrous magnesium sulfate, and evaporated under reduced pressure.
 

Historical Records

Technical Information

Categories