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Chemical Structure| 602-04-0 Chemical Structure| 602-04-0

Structure of 602-04-0

Chemical Structure| 602-04-0

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Product Details of [ 602-04-0 ]

CAS No. :602-04-0
Formula : C28H25N3
M.W : 403.52
SMILES Code : CC(N1)=C(C(C2=C(C)NC3=C2C=CC=C3)C4=C(C)NC5=C4C=CC=C5)C6=C1C=CC=C6

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Application In Synthesis of [ 602-04-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 602-04-0 ]

[ 602-04-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 95-20-5 ]
  • [ 215734-58-0 ]
  • 6,7-difluoro-2-(2-methyl-1H-indol-3-yl)quinoxaline [ No CAS ]
  • [ 602-04-0 ]
  • [ 78581-99-4 ]
YieldReaction ConditionsOperation in experiment
25%; 9% With acetic acid; at 110℃; for 35h; The reaction mixturewas evaporated in vacuo. The solid was worked up with EtOH (3-4 mL). The precipitate of tris(2-methylindol-3-yl)methane(4b) was filtered off and rinsed with EtOH. Yield 9%, mp > 300 (lit. [7] mp > 300). 1 NMR spectrum (400 MHz,DMSO-d6, , ppm, J/Hz): 1.92 (9, s, CH3), 6.09 (1, s, CH), 6.60 (3, ddd, J = 7.9, 7.2, 1.0, H-5), 6.84-6.90 (6, m,H-6, 7), 7.16 (3, dd, J = 7.9, 1.2, H-4), 10.37 (3, s, NH). Mass spectrum (EI, 70 eV), m/z (Irel, %): 404 (33), 403 (M+, 89),402 (22), 272 (75), 271 (15), 257 (86), 256 (32).
 

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