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Chemical Structure| 59489-31-5 Chemical Structure| 59489-31-5

Structure of 59489-31-5

Chemical Structure| 59489-31-5

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Product Details of [ 59489-31-5 ]

CAS No. :59489-31-5
Formula : C8H4Cl2N2
M.W : 199.04
SMILES Code : ClC1=CC=C2N=CC(Cl)=NC2=C1
MDL No. :MFCD03426386
InChI Key :YNASAKVGUCRNEP-UHFFFAOYSA-N
Pubchem ID :2758223

Safety of [ 59489-31-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302+H312+H332-H315-H319-H335
Precautionary Statements:P261-P280-P305+P351+P338

Application In Synthesis of [ 59489-31-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 59489-31-5 ]

[ 59489-31-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 59489-31-5 ]
  • [ 30757-50-7 ]
  • 2,7-bis(3,3',4,4'-tetracyanophenoxy)quinoxaline [ No CAS ]
YieldReaction ConditionsOperation in experiment
93 mmol With calcium hydride; 1,3-dimethylimidazolim iodide; at 70℃; under 3750.38 Torr; for 0.5h; 100 mmol of 2,7-dichloroquinoxaline,210 mmol of <strong>[30757-50-7]3,4-dicyanophenol</strong>,220 mol of calcium hydride and 850 mmol of iodinated 1,3-dimethylimidazole were placed in a stainless steel reaction kettle.At a pressure of 0.5 MPa and stirring conditions,The temperature of the control system is 70 C.Reaction for 30 minutes,After the system is restored to normal temperature and pressure,Pour the solution into deionized water to precipitate a solid.Recovering the ionic liquid and suctioning the resulting solid,After washing 5 times with deionized water, it was dried at 80 C for 12 hours.Recrystallized from acetonitrile,Obtaining 2,7-bis(3,3',4,4'-tetracyanophenoxy)quinoxaline 93 mmol;
 

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