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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 594-39-8 Chemical Structure| 594-39-8

Structure of 594-39-8

Chemical Structure| 594-39-8

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Product Details of [ 594-39-8 ]

CAS No. :594-39-8
Formula : C5H13N
M.W : 87.16
SMILES Code : CC(N)(C)CC
MDL No. :MFCD00008056
InChI Key :GELMWIVBBPAMIO-UHFFFAOYSA-N
Pubchem ID :68986

Safety of [ 594-39-8 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H225-H301-H314
Precautionary Statements:P210-P280-P301+P310-P305+P351+P338-P310
Class:3(8)
UN#:2924
Packing Group:

Application In Synthesis of [ 594-39-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 594-39-8 ]

[ 594-39-8 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 21279-62-9 ]
  • [ 594-39-8 ]
  • 3-(tert-pentylamino)pyrazine-2-carboxamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
51.3% With pyridine; In methanol; at 140℃; for 0.5h;Microwave irradiation; General procedure: The starting compound (1.27 mmol) was treated with 18 aliphatic amines, alicyclic amines or saturated heterocycles containing at least one nitrogen atom (2.54 mmol). Four reactions were completed by conventional heating methods. The conditions were 110 C, toluene as a solvent and pyridine (1.27 mmol) as a base. The reaction time was set to one hour. Then the reactions were completed using the microwave reactor with focused field and conditions used for syntheses were 140 C, 30 min,120 W, methanol used as a solvent and pyridine (1.27 mmol) as a base. They were set experimentally with respect to prior experience. The progress of reaction was monitored with TLC in system hexane/ethyl acetate (1:1). Then the mixture was separated by flash column chromatograph using gradient elution. Mobile phases were hexane and ethyl acetate again.
  • 2
  • [ 594-39-8 ]
  • [ 156150-67-3 ]
  • 4-(3-chloro-4-fluorophenyl)-2-methylbutan-2-amine [ No CAS ]
  • 3
  • [ 117-21-5 ]
  • [ 594-39-8 ]
  • 3-chloro-2-(tert-amylcarbamoyl)benzoic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
60% In dichloromethane; at 30℃; for 3h; Disperse <strong>[117-21-5]3-chlorophthalic anhydride</strong> (913mg) in 7.3ml of dry dichloromethane,At 30C, (A-2)-NH2 (435 mg) was slowly added to the resulting suspension and stirred for 3 h.After the completion of the reaction, the dichloromethane was spin-dried under reduced pressure and purified by silica gel chromatography (petroleum ether: ethyl acetate = 2:1) to obtain 810 mg of white solid.The yield is 60%.
 

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