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Chemical Structure| 5762-56-1 Chemical Structure| 5762-56-1

Structure of 5762-56-1

Chemical Structure| 5762-56-1

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Product Details of [ 5762-56-1 ]

CAS No. :5762-56-1
Formula : C7H19N3
M.W : 145.25
SMILES Code : CN(C(N(C)C)N(C)C)C
MDL No. :MFCD00008322

Safety of [ 5762-56-1 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H225-H314
Precautionary Statements:P210-P235-P240-P241-P242-P243-P260-P264-P280-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P321-P363-P370+P378-P403+P235-P405-P501
Class:3(8)
UN#:2733
Packing Group:

Application In Synthesis of [ 5762-56-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5762-56-1 ]

[ 5762-56-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 5762-56-1 ]
  • [ 4837-88-1 ]
  • [ 96631-91-3 ]
  • 2
  • [ 53400-41-2 ]
  • [ 5762-56-1 ]
  • [ 124-46-9 ]
  • 5,6-dihydropyrido[2,3-h]quinazolin-2-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
In methanol; water; toluene; EXAMPLE 23 5,6-Dihydropyrido[2,3-h]quinazolin-2-amine To a refluxing solution, under nitrogen, of 45.0 g (0.306 mol) of <strong>[53400-41-2]7,8-dihydro-5(6H)-quinolinone</strong>, (Example 1), in 750 ml of toluene is added dropwise a solution of 49.8 g (0.343 mol) of tris(dimethylamino)-methane in 250 ml of toluene. The solution is refluxed for 2 hours, cooled and concentrated. The residue is dissolved in 1 l of methanol and treated with 66.2 g (0.367 mol) of guanidine carbonate. The reaction mixture is refluxed, under nitrogen, for 2 hours. The mixture is concentrated to a green solid, the solid is washed with 500 ml of water, filtered and vacuum dried to give 69.1 g of crude product. Recrystallization from acetonitrile affords 6.8 g (77%) of the title compound as a light brown solid; mp 220-226 C.
 

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