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Chemical Structure| 574-61-8 Chemical Structure| 574-61-8

Structure of 574-61-8

Chemical Structure| 574-61-8

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Product Details of [ 574-61-8 ]

CAS No. :574-61-8
Formula : C19H16N2
M.W : 272.34
SMILES Code : C1(NN=C(C2=CC=CC=C2)C3=CC=CC=C3)=CC=CC=C1
MDL No. :MFCD00046773

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Application In Synthesis of [ 574-61-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 574-61-8 ]

[ 574-61-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 451-40-1 ]
  • [ 574-61-8 ]
  • [ 3469-20-3 ]
YieldReaction ConditionsOperation in experiment
85% With toluene-4-sulfonic acid; In ethanol; toluene; for 12h;Reflux; Intermediate 1-3 (20 g 73.47 mmol) and diphenyl ethyl ketone (14.40 g 73.47 mmol) were added to a mixed solvent of toluene and ethanol (500 mL Vtoluene: VEtOH = 4:1), followed by p-toluenesulfonic acid ( 63.25g 367.35mmol), refluxing reaction for 12h, after completion of the reaction, the mixture was washed with water, extracted with DCM, dried with organic phase and purified by silica gel column chromatography to afford intermediate 1-5 (16.8 g, 85%), MW: 269.12.
 

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