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Chemical Structure| 56946-83-9 Chemical Structure| 56946-83-9

Structure of 56946-83-9

Chemical Structure| 56946-83-9

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Product Details of [ 56946-83-9 ]

CAS No. :56946-83-9
Formula : C4HCl3O2S2
M.W : 251.54
SMILES Code : O=S(C1=C(Cl)SC(Cl)=C1)(Cl)=O
MDL No. :MFCD00051665
InChI Key :JJKSHSHZJOWSEC-UHFFFAOYSA-N
Pubchem ID :2736094

Safety of [ 56946-83-9 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314
Precautionary Statements:P280-P305+P351+P338-P310
Class:8
UN#:1760
Packing Group:

Application In Synthesis of [ 56946-83-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 56946-83-9 ]

[ 56946-83-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 56946-83-9 ]
  • [ 120-35-4 ]
  • 3-(2,5-Dichloro-thiophene-3-sulfonylamino)-4-methoxy-N-phenyl-benzamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
Example 132 3-(2,5-Dichlorothiophene-3-sulfonylamino)-4-methoxy-N-phenyl-benzamide Prepared according to the procedure described for Example 127 using 2,5-dichlorothiophene-3-sulfonyl chloride (0.75 g, 3.0 mmol) and 3-amino-4-methoxy-N-phenyl-benzamide (0.73 g, 3.0 mmol) to afford the product (0.9 g); m.p. 189-190 C. Calculated for C18H14Cl2N2O4S2: C, 47.27; H, 3.09; N, 6.13. Found: C, 47.51; H, 3.04; N, 5.91.
  • 2
  • [ 56946-83-9 ]
  • [ 31785-05-4 ]
  • C11H10Cl2N2O4S3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
60 mg Intermediate 50 Sodium hydride (60% disp. in oil; 48mg, 1.21 mmol) was suspended in dry tetrahydrofuran (5ml_) under nitrogen. To this, 5-amino-2-methyl-thiazole-4- carboxylic acid ethyl ester (150mg, 0.806mmol) was added at 0C and the mixture was stirred for 15 minutes. To this, 2,5-dichlorothiophene-3-sulfonyl chloride (243mg, 0.967mmol) was added at 0C and the mixture stirred at room temperature for 4 hours. Water was added to the reaction mixture at 0C and the mixture concentrated in vacuo. The residue was purified by preparative TLC eluting with 100% ethyl acetate to give Intermediate 50 (60mg) as an off white solid. LCMS (Method 33) Rt 1.91 min; m/z(M+H)+ 401
 

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