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Chemical Structure| 5622-49-1 Chemical Structure| 5622-49-1

Structure of 5622-49-1

Chemical Structure| 5622-49-1

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Product Details of [ 5622-49-1 ]

CAS No. :5622-49-1
Formula : C11H13NO2
M.W : 191.23
SMILES Code : O=C(O)CC1=CC2=C(NCCC2)C=C1

Safety of [ 5622-49-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 5622-49-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5622-49-1 ]

[ 5622-49-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 5622-49-1 ]
  • [ 18107-18-1 ]
  • [ 5622-50-4 ]
YieldReaction ConditionsOperation in experiment
In dichloromethane; at 0℃; To a suspension of 2-(1,2,3, 4-tetrahydroquinolin-6-yl)acetic acid (1 g, 5.23 mmol) in DCM (5 ml) at 0 C was added trimethylsilyldiazomethane in hexane (7.84 ml, 15.69 mmol) dropwise. Gas was evolved from the reaction mixture during the addition. After the completion of addition, the mixture was concentrated and purified using flash column chromatography (eluting with hexane/ethyl acetate: ethanol = 3: 1, starting with 100% hexane, end with 20% hexane) to give the desired product as an oil. LCMS m/z (M+H) calc'd: 206.1 ; found: 206.1.
 

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