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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 55930-23-9 Chemical Structure| 55930-23-9

Structure of 55930-23-9

Chemical Structure| 55930-23-9

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Product Details of [ 55930-23-9 ]

CAS No. :55930-23-9
Formula : C8H13ClO
M.W : 160.64
SMILES Code : O=C(Cl)[C@H]1CC[C@H](C)CC1
MDL No. :MFCD17012702

Safety of [ 55930-23-9 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H311+H331-H314
Precautionary Statements:P310-P260-P280
Class:8(6.1)
UN#:2922
Packing Group:

Application In Synthesis of [ 55930-23-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 55930-23-9 ]

[ 55930-23-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 942589-45-9 ]
  • [ 55930-23-9 ]
  • [ 1027708-01-5 ]
YieldReaction ConditionsOperation in experiment
In 1,2-dichloro-ethane; for 3h;Heating / reflux; Intermediate 9Methyl 5-iodo-3-[(frans-4-methylcyclohexyl)carbonyl]amino}-2-thiophenecarboxylateTo a mixture of methyl S-amino-delta-iodo^-thiophenecarboxylate (Intermediate 8) (0.54 g) in DCE (25 ml.) was added frans-4-methylcyclohexanecarbonyl chloride1 (910 mg, 5.7 mmol) and the mixture heated under reflux under nitrogen for 3 h. The mixture was cooled, water (20 ml.) was added, and after stirring for 5 mins, the mixture was passed through a hydrophobic frit. The aqueous layer was extracted twice with DCM, the organic fractions combined, dried (hydrophobic frit) and evaporated. The crude material was purified by ISCO Companion silica chromatography, eluting with a gradient 0-50% DCM in cyclohexane to give the title compound. MS calcd for (C14H18INO3S + H)+: 408 MS found (electrospray): (M+H)+ = 408
 

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