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[ CAS No. 5389-87-7 ] {[proInfo.proName]}

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Chemical Structure| 5389-87-7
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Product Details of [ 5389-87-7 ]

CAS No. :5389-87-7 MDL No. :MFCD00000983
Formula : C10H17Cl Boiling Point : -
Linear Structure Formula :- InChI Key :WLAUCMCTKPXDIY-JXMROGBWSA-N
M.W : 172.70 Pubchem ID :6372219
Synonyms :

Safety of [ 5389-87-7 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P210-P261-P264-P271-P280-P302+P352-P304+P340+P312-P305+P351+P338-P332+P313-P337+P313-P362-P370+P378-P403+P233-P403+P235-P405-P501 UN#:N/A
Hazard Statements:H227-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 5389-87-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 5389-87-7 ]
  • Downstream synthetic route of [ 5389-87-7 ]

[ 5389-87-7 ] Synthesis Path-Upstream   1~4

  • 1
  • [ 93-35-6 ]
  • [ 5389-87-7 ]
  • [ 495-02-3 ]
Reference: [1] Phytochemistry, 2004, vol. 65, # 22, p. 3021 - 3027
  • 2
  • [ 106-24-1 ]
  • [ 98-88-4 ]
  • [ 6138-90-5 ]
  • [ 94-48-4 ]
  • [ 5389-87-7 ]
YieldReaction ConditionsOperation in experiment
67 %Spectr. With 1-pyrrolidinecarboxaldehyde; sodium bromide In acetone at 0 - 20℃; for 20.5 h; General procedure: In the presence of 2.5 molpercent FPyr allylic bromide 8 was synthesized with BzCI (1.2 equiv) according to general procedure VIII (chapter 4.9.1, t = 20 h) in 67percent yield as shown by internal standard (ratio oflinear and branched regioisomer of 98:2). Besides chloride 24 was obtained in 7percent yield (ratio bromide 84/chloride 24 91:9) together with geranyl benzoate E-34 in 12percent yield (ratio 84+24/34 86:14).
Reference: [1] Patent: WO2016/202894, 2016, A1, . Location in patent: Page/Page column 182; 183; 184
  • 3
  • [ 106-24-1 ]
  • [ 6138-90-5 ]
  • [ 5389-87-7 ]
Reference: [1] Organic Letters, 2018, vol. 20, # 10, p. 2980 - 2983
  • 4
  • [ 5389-87-7 ]
  • [ 6138-90-5 ]
Reference: [1] Journal of Organic Chemistry, 1982, vol. 47, # 25, p. 4955 - 4963
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