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Chemical Structure| 5335-84-2 Chemical Structure| 5335-84-2

Structure of 5335-84-2

Chemical Structure| 5335-84-2

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Product Details of [ 5335-84-2 ]

CAS No. :5335-84-2
Formula : C12H8Br2S2
M.W : 376.13
SMILES Code : BrC1=CC=C(SSC2=CC=C(Br)C=C2)C=C1
MDL No. :MFCD00017832
InChI Key :VZQVHIINDXJOQK-UHFFFAOYSA-N
Pubchem ID :219553

Safety of [ 5335-84-2 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H315-H318-H335-H410
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P310-P332+P313-P362-P403+P233-P405-P501-P273-P391
Class:8
UN#:1759
Packing Group:

Application In Synthesis of [ 5335-84-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5335-84-2 ]

[ 5335-84-2 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 67-64-1 ]
  • [ 98-58-8 ]
  • palladium [ No CAS ]
  • [ 5335-84-2 ]
  • [ 1195-33-1 ]
  • 2
  • [ 422-64-0 ]
  • [ 5335-84-2 ]
  • [ 782491-17-2 ]
  • 3
  • [ 5335-84-2 ]
  • [ 157869-15-3 ]
  • [ 1285494-88-3 ]
YieldReaction ConditionsOperation in experiment
86% With copper(l) iodide; caesium carbonate; In dimethyl sulfoxide; at 80℃; A mixture of 2-alkynylaniline 1a-1e (0.2 mmol), dichalcogenide 2a-2e (0.15 mmol), CuI (0.02 mmol), and Cs2CO3 (0.2 mmol) in DMSO (2 mL) was stirred at 80 C under an air atmosphere. After completion of the reaction that was monitored by GC-MS or TLC, 25 mL water was added, and the mixture was extracted with ethyl acetate, the combined organic layers were washed with water (10 mL x 3), dried over anhydrous Na2SO4. After filtration and removal of solvents in vacuum, the residue was purified by silica gel column chromatography to afford the corresponding products.
  • 4
  • [ 93-89-0 ]
  • [ 5335-84-2 ]
  • [ 30506-30-0 ]
 

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