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Chemical Structure| 5326-27-2 Chemical Structure| 5326-27-2

Structure of 5326-27-2

Chemical Structure| 5326-27-2

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Product Details of [ 5326-27-2 ]

CAS No. :5326-27-2
Formula : C7H8N2O2
M.W : 152.15
SMILES Code : NNC1=CC=CC=C1C(O)=O
MDL No. :MFCD00129768

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Application In Synthesis of [ 5326-27-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5326-27-2 ]

[ 5326-27-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1218-69-5 ]
  • [ 5326-27-2 ]
  • [ 201530-78-1 ]
YieldReaction ConditionsOperation in experiment
In ethanol; EXAMPLE 41 2-[3,5Bis(2-hydroxyphenyl)-[1,2,4]triazol-1-yl]benzoic acid 4.8 g of 2-(2-hydroxyphenyl)benz[e][1,3]oxazin4-one and 3.5 g of 2-hydrazinobenzoic acid are boiled under reflux for 4 h in 10 ml of ethanol. The mixture is cooled, poured onto water and extracted with ethyl acetate. The combined organic phases are dried over sodium sulfate and concentrated on a rotary evaporator. The residue is crystallized from ethyl acetate/hexane. After drying, 2-[3,5-bis(2-hydroxyphenyl)-[1,2,4]triazol-1-yl]benzoic acid is obtained as colorless crystals of m.p. 132-138 C.
 

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