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There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.

Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic USD 100+
Accessible (Haz class 3, 4, 5 or 8), International USD 200+
Chemical Structure| 53199-31-8 Chemical Structure| 53199-31-8
Chemical Structure| 53199-31-8
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Product Details of [ 53199-31-8 ]

CAS No. :53199-31-8
Formula : C24H54P2Pd
M.W : 511.05
SMILES Code : CC(P(C(C)(C)C)C(C)(C)C)(C)C.CC(P(C(C)(C)C)C(C)(C)C)(C)C.[Pd]
MDL No. :MFCD03094580
InChI Key :MXQOYLRVSVOCQT-UHFFFAOYSA-N
Pubchem ID :2734558

Safety of [ 53199-31-8 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H315-H319-H228
Precautionary Statements:P240-P210-P241-P264-P280-P302+P352-P370+P378-P337+P313-P305+P351+P338-P362+P364-P332+P313
Class:4.1
UN#:1325
Packing Group:

Application In Synthesis [ 53199-31-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 53199-31-8 ]

[ 53199-31-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 52522-40-4 ]
  • [ 131274-22-1 ]
  • [ 53199-31-8 ]
YieldReaction ConditionsOperation in experiment
80% With sodium methylate; dimethyl sulfoxide; In methanol; at 50℃; for 15h;Inert atmosphere; Under inert gas protection,Tri-tert-butylphosphonium tetrafluoroborate (9.3 g, 0.032 mil,4Eq), tris (dibenzylideneacetone) dipalladium () chloroform adduct (8. 3g, 008 mol, leq) and 200 mlDimethyl sulfoxide was added to the reaction flask,And then slowly dropping to them1M sodium methoxide solution in methanol(32L, 0.032, 0e, 4eq),50 ° C for 15 h.Gloves bag filter,The filter cake was washed with dimethyl sulfoxideThe The filter cake was dried in n-hexane.filter,The filtrate was concentrated and crystallized.filter,The filter cake was washed with a small amount of n-hexane and the filter cake was washed with a small amount of n-hexane and dried to give 3. 27 g of a white solid powder in 80percent yield, elemental analysis: C, 56.17;H, 10. 50; P, 12. 07; Pd, 21.26
  • 2
  • [ 52409-22-0 ]
  • [ 131274-22-1 ]
  • [ 53199-31-8 ]
 

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