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Chemical Structure| 52387-36-7 Chemical Structure| 52387-36-7

Structure of 6-chlorohexanal
CAS No.: 52387-36-7

Chemical Structure| 52387-36-7

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Product Details of [ 52387-36-7 ]

CAS No. :52387-36-7
Formula : C6H11ClO
M.W : 134.60
SMILES Code : O=CCCCCCCl
MDL No. :MFCD12031784
InChI Key :GVIQYWPEJQUXLX-UHFFFAOYSA-N
Pubchem ID :643049

Safety of [ 52387-36-7 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301-H315-H318-H335
Precautionary Statements:P280-P301+P310+P330-P302+P352-P305+P351+P338+P310
Class:6.1
UN#:2810
Packing Group:

Application In Synthesis of [ 52387-36-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 52387-36-7 ]

[ 52387-36-7 ] Synthesis Path-Downstream   1~5

  • 3
  • [ 52387-36-7 ]
  • [ 4224-62-8 ]
  • [ 1233324-43-0 ]
  • 4
  • [ 52387-36-7 ]
  • [ 78834-75-0 ]
  • 5
  • [ 52387-36-7 ]
  • [ 4224-62-8 ]
YieldReaction ConditionsOperation in experiment
81% With N-hydroxyphthalimide; oxygen; In acetonitrile; at 30℃; for 3h;Schlenk technique; 15 molpercent NHPI was added to a 25 mL Schlenk reaction tube, dried under vacuum for 15 minutes, oxygen was bubbled in, and 2 mL of acetonitrile and 1.0 equivalent of 6-chlorohexanal were added in an oxygen atmosphere, and an oxygen balloon was attached thereto, and a glass stopper was added to the reaction tube. After that, it was placed in an oil bath and reacted at 30 ° C for 3 h. After the completion of the reaction, the mixture was concentrated under reduced pressure and purified by column chromatography, eluting with petroleum ether / ethyl acetate / methylene chloride (v: v: v = 5:1:1) to give 6-chlorohexanoic acid. Yield 81percent,Colorless liquid
 

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