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Chemical Structure| 4830-93-7 Chemical Structure| 4830-93-7

Structure of 4830-93-7

Chemical Structure| 4830-93-7

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Product Details of [ 4830-93-7 ]

CAS No. :4830-93-7
Formula : C10H13Cl
M.W : 168.66
SMILES Code : ClCCCCC1=CC=CC=C1
MDL No. :MFCD00037117

Safety of [ 4830-93-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 4830-93-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 4830-93-7 ]

[ 4830-93-7 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 4830-93-7 ]
  • [ 99-96-7 ]
  • [ 30131-16-9 ]
YieldReaction ConditionsOperation in experiment
85.2% With potassium carbonate; In 5,5-dimethyl-1,3-cyclohexadiene; at 130 - 140℃; for 24h;Inert atmosphere; Into a 500 ml four-necked flask, nitrogen was added for protection, and 75 g of 1-chloro-4-phenylbutane, 69 g of p-hydroxybenzoic acid, 65 g of potassium carbonate, 175 g of xylene, and 0.75 g of polyethylene glycol were added. After refluxing at 130~140 C for 24h, after high-performance liquid chromatography (HPLC), the temperature is lowered to room temperature, 1~5% liquid alkali is added for washing, xylene is concentrated, methanol is added to dissolve, and the reaction temperature is adjusted to be less than At 20 C, filtration, partial concentration of methanol, and filtration under reduced temperature gave p-butoxybenzoic acid with a molar yield of 85.2% and a purity of 98.56% (detected by high performance liquid chromatography (HPLC)). The synthesis process in the embodiment is simple in steps and convenient in operation, and avoids the production of the highly toxic intermediate phenylbutane bromide and a large amount of waste water in the synthesis process, so that the environment is friendly and the production cost is saved, and the pair obtained by the process is synthesized. Phenylbutoxybenzoic acid has high purity and is suitable for large-scale industrial production
 

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