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Chemical Structure| 4773-35-7 Chemical Structure| 4773-35-7

Structure of 4773-35-7

Chemical Structure| 4773-35-7

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Product Details of [ 4773-35-7 ]

CAS No. :4773-35-7
Formula : C9H9ClO
M.W : 168.62
SMILES Code : CC(C(Cl)C1=CC=CC=C1)=O
MDL No. :MFCD04614623

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Application In Synthesis of [ 4773-35-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 4773-35-7 ]

[ 4773-35-7 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 4773-35-7 ]
  • [ 17356-08-0 ]
  • [ 30709-67-2 ]
  • 2
  • [ 214834-18-1 ]
  • [ 4773-35-7 ]
  • C20H26N2O2S [ No CAS ]
YieldReaction ConditionsOperation in experiment
With sodium acetate; acetic acid; at 80℃; 2.5 g of Intermediate V (0.01 mol), 1.7 g of Intermediate III (0.01 mol), 1.7 g of anhydrous sodium acetate (0.02 mol), acetic acid 30 mL were added to a 100 mL three-necked flask, and the reaction was stirred at 80 C overnight. The reaction solution was filtered and desalted, spun dry, dissolved in 50 mL of dichloromethane, and then added to 50 mL of water. After separation, the dichloromethane was taken, and the aqueous layer was extracted twice with 50 mL of dichloromethane. Yellow oily liquid. Add 4 mL of 4N HCl/dioxane, stir at room temperature for 2 h, and filter to give a white solid. drying gives compound VII.
 

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