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Chemical Structure| 460347-59-5 Chemical Structure| 460347-59-5

Structure of 460347-59-5

Chemical Structure| 460347-59-5

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Product Details of [ 460347-59-5 ]

CAS No. :460347-59-5
Formula : C26H25BO2
M.W : 380.29
SMILES Code : CC1(C)OB(OC(C)1C)C2=C3C(C=CC=C3)=C(C4=CC=CC=C4)C5=CC=CC=C25
MDL No. :MFCD13194955
InChI Key :MVGDRHFJGXEKBG-UHFFFAOYSA-N
Pubchem ID :59207618

Safety of [ 460347-59-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 460347-59-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 460347-59-5 ]

[ 460347-59-5 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 460347-59-5 ]
  • [ 74137-36-3 ]
  • C47H32O [ No CAS ]
YieldReaction ConditionsOperation in experiment
66% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In ethanol; water; toluene; at 110℃; for 24h;Inert atmosphere; 4) (Suzuki) by Suzuki coupling reaction to obtain the final product c: the 9 - benzene anthracene -10 borate 10 mmol, 1, 3 - dibromo - 4, 6 - dihydro -5 - methoxybenzene 2 mmol, four (triphenylphosphine) palladium 0.4 mmol, toluene 80 ml, ethanol 20 ml, K2CO344 MmoL (for 20 ml distilled water into the solution), is added to the reaction bottle, then the system vacuum, in 110 °C under the protection of nitrogen reflux 24 hours. After the completion of the reaction, methanol hot washing and filtering, toluene recrystallization, distillation to obtain the final product c. Yield 66percent.
  • 2
  • [ 460347-59-5 ]
  • [ 59785-43-2 ]
  • C48H34 [ No CAS ]
YieldReaction ConditionsOperation in experiment
66% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In ethanol; water; toluene; at 110℃; for 24h;Inert atmosphere; (4) (Suzuki) by Suzuki coupling reaction to obtain the final product d: the 9 - benzene anthracene -10 borate 10 mmol, 1, 3 - dibromo - 4, 6 - dihydro -5 - ethyl 2 mmol, four (triphenylphosphine) palladium 0.4 mmol, toluene 80 ml, ethanol 20 ml, K2CO344 MmoL (for 20 ml distilled water into the solution), is added to the reaction bottle, then the system vacuum, in 110 C under the protection of nitrogen reflux 24 hours. After the completion of the reaction, methanol hot washing and filtering, toluene recrystallization, distillation to obtain the final product d. Yield 66%.
 

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