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Chemical Structure| 41994-92-7 Chemical Structure| 41994-92-7

Structure of 41994-92-7

Chemical Structure| 41994-92-7

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Product Details of [ 41994-92-7 ]

CAS No. :41994-92-7
Formula : C8H8N2O4
M.W : 196.16
SMILES Code : O=C(N)C1=CC(OC)=CC=C1[N+]([O-])=O
MDL No. :MFCD07780729

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 41994-92-7 ]

[ 41994-92-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 41994-92-7 ]
  • [ 38469-84-0 ]
YieldReaction ConditionsOperation in experiment
92% With triethylamine; trifluoroacetic anhydride; In dichloromethane; at 20℃; for 1h; Step 2 5-Methoxy-2-nitrobenzonitrile A 100 mL round bottom flask was charged with 5-methoxy-2-nitrobenzamide (2.1 g, 0.01 mol), trifluoroacetic anhydride (2.2 mL), triethylamine (2.9 mL) and CH2Cl2 (30 mL). The resulting solution was stirred at room temperature for 1 h. Work-up: the reaction solution was washed with H2O (30 mL*2). The organic layer was dried over anhydrous Na2SO4 and concentrated in vacuo, to give 1.75 g (92%) of the product as white solid. MS m/z: 179 (M+H+).
 

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